Article: Physical aging kinetics of syndiotactic polystyrene as determined from creep behavior.

INTRODUCTION

The cooling of an amorphous polymer through the glass transition [T.sub.g] results in a non-equilibrium glassy state that then proceeds to spontaneously evolve towards a temporally distant equilibrium (1, 2). Associated with the evolution of the state variables of, e.g., volume or enthalpy, are observable changes of macroscopic properties such as viscoelastic response, yield strength, impact resistance, etc. (3), which has come to be referred to as physical aging. One anticipates similar behavior for the glassy response of semicrystalline polymers. However, it has been observed that for semicrystalline polymers physical aging persists even above the ...

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