Article: Protected and Activated Amino Acids.

Jean-Pierre Senet is R&D director for Isochem, the wholly-owned subsidiary of the Groupe SNPE.

The protection of amines as their alkyloxycarbonyl derivatives is widely used in peptide synthesis. Some of the most common alkyloxycarbonyl N-protecting groups employed for the protection of amino acids include: benzyloxycarbonyl (Z or Cbz) t-butoxycarbonyl (Boc), 9-fluorenyl-methoxycarbonyl (Emoc) and-4-nitro benzyloxy-carbonyl. These protecting groups are often introduced on amino acids or peptides with alkyl chloroformates, provided they are easily available and sufficiently stable to be safely handled.

Thus, benyzl chloroformate (Z-CI)is a unique reagent ...

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