Article: Microbeam characterization of Corning archeological reference glasses: New additions to the Smithsonian microbeam standard collection.

An initial study of the minor element, trace element, and impurities in Corning archeological references glasses have been performed using three microbeam techniques: electron probe microanalysis (EMPMA), laser ablation ICP-mass spectrometry (LA ICP-MS), and secondary ion mass spectrometry (SIMS). The EPMA results suggest a significant level of heterogeneity for a number of metals. Conversely, higher precision and a larger sampling volume analysis by LA ICP-MS indicates a high degree of chemical uniformity within all glasses, typically

Key words: chemical heterogeneity; electron probe microanalysis; glass; laser ablation ICP-MS; microbeam; microscale characterization; ...

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