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Analysis of Volatile and Semivolatile Organic Compounds in Municipal Wastewater Using Headspace Solid-Phase Microextraction and Gas Chromatography
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Water Environment Research
- Article date:
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August 1, 2007
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Copyright informationCopyright Water Environment Federation Aug 2007. Provided by ProQuest LLC. (Hide copyright information)
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ABSTRACT:
The aim of this work was to develop a simple and fast analytical method for the determination of a wide range of organic compounds (volatile and semivolatile compounds) in municipal wastewater. The headspace-solid-phase microextraction (HS-SPME) and gas chromatography (with mass spectroscopy) was used for determination of the organic compounds. In this study, 39 organic compounds were determined, including 3 sulfur compounds, 28 substituted benzenes, and 8 substituted phenols. The extraction parameters, such as types of SPME fiber, extraction temperature, extraction time, desorption time, salt effect, and magnetic stirring, were investigated. The method had very good ...
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